4BSO

Crystal structure of R-spondin 1 (Fu1Fu2) - Native

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	I 2 2 2
Unit cell lengths	37.160, 63.900, 92.460
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.480 - 2.200
R-factor	0.2139
Rwork	0.212
R-free	0.24990
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.021
RMSD bond angle	2.124
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	34.400
High resolution limit [Å]	2.200
Rmerge	0.100
Number of reflections	5873
<I/σ(I)>	11.1
Completeness [%]	100.0
Redundancy	7.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1