4BSD
Human H7N9 Influenza Virus Haemagglutinin (with Asn-133 Glycosylation) in Complex with Avian Receptor Analogue 3'-SLN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | H 3 2 |
Unit cell lengths | 115.950, 115.950, 295.380 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 59.560 - 2.400 |
R-factor | 0.23887 |
Rwork | 0.237 |
R-free | 0.27691 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ti8 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.032 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 59.560 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.060 | 0.510 |
Number of reflections | 30146 | |
<I/σ(I)> | 10.37 | 1 |
Completeness [%] | 99.4 | 98.9 |
Redundancy | 3.9 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 291 | 291 K, 0.1 M PIPES PH 7.0, 2.2 M AMMONIUM SULFATE, 1% PEG 400 |