4BRY
The Idas:Geminin heterodimeric parallel coiled-coil
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-02-04 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 117.799, 117.799, 103.462 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.946 - 2.890 |
R-factor | 0.204 |
Rwork | 0.203 |
R-free | 0.22600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1uii |
RMSD bond length | 0.019 |
RMSD bond angle | 2.296 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.950 | 3.050 |
High resolution limit [Å] | 2.890 | 2.890 |
Rmerge | 0.130 | 0.840 |
Number of reflections | 8415 | |
<I/σ(I)> | 9.8 | 2.3 |
Completeness [%] | 99.8 | 99.5 |
Redundancy | 6.3 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.1 M SPG PH 7.5, 10 % ISOPROPANOL |