4BRO
Legionella pneumophila NTPDase1 crystal form IV (part-open)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.2 |
Synchrotron site | BESSY |
Beamline | 14.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Spacegroup name | P 63 |
Unit cell lengths | 155.991, 155.991, 79.222 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.170 - 1.990 |
R-factor | 0.21509 |
Rwork | 0.215 |
R-free | 0.24069 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.526 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.140 |
Number of reflections | 74335 |
<I/σ(I)> | 6.9 |
Completeness [%] | 99.1 |
Redundancy | 5.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 100MM HEPES PH 7.5, 1.4 M (NH4)2SO4 |