4BOU
Structure of OTUD3 OTU domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 287 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 32 1 2 |
Unit cell lengths | 36.196, 36.196, 211.051 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 31.347 - 1.550 |
R-factor | 0.1771 |
Rwork | 0.175 |
R-free | 0.22860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3pfy |
RMSD bond length | 0.005 |
RMSD bond angle | 0.916 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.210 | 1.630 |
High resolution limit [Å] | 1.550 | 1.550 |
Rmerge | 0.040 | 0.480 |
Number of reflections | 23429 | |
<I/σ(I)> | 14.9 | 2.1 |
Completeness [%] | 98.9 | 99.1 |
Redundancy | 3.9 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10% PEG 4K, 0.1 M KCL, 0.01 M MGCL2, 50 MM MES PH 6.0 |