4BMG
Crystal structure of hexameric HBc149 Y132A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2013-02-06 |
Detector | DECTRIS PILATUS 2M-F |
Spacegroup name | P 1 |
Unit cell lengths | 64.790, 67.750, 86.610 |
Unit cell angles | 68.98, 70.75, 84.51 |
Refinement procedure
Resolution | 44.526 - 3.000 |
R-factor | 0.2555 |
Rwork | 0.252 |
R-free | 0.31730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kxs |
RMSD bond length | 0.010 |
RMSD bond angle | 1.450 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.690 | 3.080 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.030 | 0.430 |
Number of reflections | 24745 | |
<I/σ(I)> | 17.2 | 1.8 |
Completeness [%] | 95.3 | 94 |
Redundancy | 1.8 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 293 | 100 MM CITRATE PH 5.0, 15 % (V/V) ISO-PROPANOL, 1% (W/V) PEG 10 000, 293 K |