4BM9
Structure of the autoinhibited Parkin catalytic domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-02-10 |
Detector | DECTRIS PIXEL |
Spacegroup name | H 3 2 |
Unit cell lengths | 168.420, 168.420, 97.181 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.619 - 2.250 |
R-factor | 0.1918 |
Rwork | 0.190 |
R-free | 0.21780 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.974 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | SHELX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 58.330 | 2.370 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.090 | 0.640 |
Number of reflections | 24502 | |
<I/σ(I)> | 10.3 | 2.3 |
Completeness [%] | 98.0 | 99.1 |
Redundancy | 5 | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 1.6 M LITHIUM SULPHATE, 10 MM MAGNESIUM CHLORIDE, 50 MM MES (PH 5.4) |