4BM5
Chloroplast inner membrane protein TIC110
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 121.100, 121.100, 242.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 27.370 - 4.200 |
R-factor | 0.35 |
Rwork | 0.350 |
R-free | 0.36600 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 2.500 |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 4.200 |
Rmerge | 0.100 |
Number of reflections | 8171 |
<I/σ(I)> | 27.8 |
Completeness [%] | 99.7 |
Redundancy | 12.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |