4BLX
CRYSTAL STRUCTURE OF FUNGAL VERSATILE PEROXIDASE I FROM PLEUROTUS OSTREATUS - CRYSTAL FORM IV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-06 |
Detector | DECTRIS PILATUS |
Spacegroup name | P 43 |
Unit cell lengths | 94.670, 94.670, 38.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.335 - 1.249 |
R-factor | 0.1607 |
Rwork | 0.160 |
R-free | 0.17930 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fmu |
RMSD bond length | 0.012 |
RMSD bond angle | 1.536 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.320 |
High resolution limit [Å] | 1.250 | 1.250 |
Rmerge | 0.090 | 1.260 |
Number of reflections | 94526 | |
<I/σ(I)> | 17.8 | 1.9 |
Completeness [%] | 99.3 | 95.7 |
Redundancy | 12.6 | 11.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20 % PEG 3350, 0.2 M AMMONIUM FORMATE. |