4BLK
Crystal Structure of Fungal Versatile Peroxidase I from Pleurotus ostreatus - Crystal Form I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS |
Synchrotron site | SLS |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-06 |
Detector | DECTRIS PILATUS |
Spacegroup name | P 43 |
Unit cell lengths | 96.500, 96.500, 38.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.156 - 1.049 |
R-factor | 0.1308 |
Rwork | 0.130 |
R-free | 0.13690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fmu |
RMSD bond length | 0.008 |
RMSD bond angle | 1.288 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.110 |
High resolution limit [Å] | 1.050 | 1.050 |
Rmerge | 0.070 | 0.860 |
Number of reflections | 156095 | |
<I/σ(I)> | 19.3 | 1.2 |
Completeness [%] | 94.3 | 66.9 |
Redundancy | 11 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M NA-ACETATE PH 4.6, 8% PEG 4000. |