4BKN
Human Dihydropyrimidinase-related protein 3 (DPYSL3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-01-31 |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 144.230, 96.650, 119.270 |
Unit cell angles | 90.00, 137.26, 90.00 |
Refinement procedure
Resolution | 42.890 - 2.100 |
R-factor | 0.19946 |
Rwork | 0.197 |
R-free | 0.23813 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vm8 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.302 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | CCP4 |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.850 | 2.150 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.180 | 0.450 |
Number of reflections | 60144 | |
<I/σ(I)> | 5.6 | 2.9 |
Completeness [%] | 93.0 | 94.2 |
Redundancy | 5.8 | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8.5 | 0.2M KSCN; 0.1M BISTRISPROPANE PH 8.5; 20% PEG 3350 10% ETHYLENE GLYCOL |