4BJJ
Sfc1-Sfc7 dimerization module
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-07-14 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 85.245, 85.245, 154.108 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.290 - 2.400 |
R-factor | 0.183 |
Rwork | 0.181 |
R-free | 0.22360 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.237 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | SHARP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.620 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.110 | 0.890 |
Number of reflections | 13629 | |
<I/σ(I)> | 14.5 | 2.1 |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 12.1 | 9.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 1.4 M AMSO4, 0.1 M HEPES PH 7, 0.1 M KCL |