4BJ6
Crystal structure Rif2 in complex with the C-terminal domain of Rap1 (Rap1-RCT)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-09-19 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 108.250, 112.680, 140.790 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.790 - 3.260 |
R-factor | 0.1731 |
Rwork | 0.172 |
R-free | 0.19530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 4BJ1 AND 3OWT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.120 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.800 | 3.270 |
High resolution limit [Å] | 3.260 | 3.260 |
Rmerge | 0.050 | 0.500 |
Number of reflections | 27519 | |
<I/σ(I)> | 22.1 | 3.2 |
Completeness [%] | 99.8 | 99.8 |
Redundancy | 4.1 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 22-25% PEG 6000, 100 MM TRIS/HCL PH 8.0, 500 MM LI2SO4 |