4BIM
CATALASE 3 FROM NEUROSPORA CRASSA IN TETRAGONAL FORM EXPOSES A MODIFIED TETRAMERIC ORGANIZATION
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-08-23 |
Detector | RIGAKU RAXIS IV PLUS PLUS |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 207.508, 207.508, 137.041 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.300 - 2.950 |
R-factor | 0.2678 |
Rwork | 0.255 |
R-free | 0.30440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ej6 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.110 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.110 | 0.460 |
Number of reflections | 62655 | |
<I/σ(I)> | 9.7 | 2.8 |
Completeness [%] | 99.3 | 98 |
Redundancy | 4.1 | 4.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | MES 100 MM, PH 5.5, 50 % V/V MPD |