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4BFM

The crystal structure of mouse PK38

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-17A
Synchrotron sitePhoton Factory
BeamlineBL-17A
Temperature [K]100
Detector technologyCCD
DetectorADSC QUANTUM 4r
Spacegroup nameP 21 21 21
Unit cell lengths35.799, 75.711, 128.088
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution48.896 - 2.350
R-factor0.1767
Rwork0.175
R-free0.20820
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3ZGW
RMSD bond length0.009
RMSD bond angle1.213
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.390
High resolution limit [Å]2.4002.350
Rmerge0.1000.360
Number of reflections15230
<I/σ(I)>35.786.21
Completeness [%]99.899.1
Redundancy10.87
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1

227561

PDB entries from 2024-11-20

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