4BFE
Structure of the extracellular portion of mouse CD200RLa
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-07 |
Detector | ADSC CCD |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 157.590, 157.590, 167.940 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.500 |
R-factor | 0.1731 |
Rwork | 0.171 |
R-free | 0.20530 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.230 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | BUSTER (2.11.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 168.020 | 2.630 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.070 | 0.490 |
Number of reflections | 42242 | |
<I/σ(I)> | 13 | 2.2 |
Completeness [%] | 98.4 | 99.7 |
Redundancy | 3.6 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 2.0M AMMONIUM SULFATE, 0.1M SODIUM CACODYLATE, 0.2M SODIUM CHLORIDE, pH 6.5 |