4BEZ
Night blindness causing G90D rhodopsin in the active conformation
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | H 3 2 |
Unit cell lengths | 242.440, 242.440, 110.360 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 3.300 |
R-factor | 0.2299 |
Rwork | 0.229 |
R-free | 0.24430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4a4m |
RMSD bond length | 0.011 |
RMSD bond angle | 1.601 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (MR) |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.470 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.310 | |
Number of reflections | 18833 | |
<I/σ(I)> | 9 | 1.43 |
Completeness [%] | 99.4 | 97.4 |
Redundancy | 20.2 | 20.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |