4B92
Crystal structure of truncated human CRMP-5 soaked with Zn
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 89.500, 89.500, 246.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.920 - 2.900 |
R-factor | 0.19377 |
Rwork | 0.191 |
R-free | 0.25009 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4b91 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.459 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.300 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.140 | 0.650 |
Number of reflections | 23108 | |
<I/σ(I)> | 10.1 | 2.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 7 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5 | 23% (V/V) PEG 400 MMT PH 5.0 |