4B8P
rImp_alpha_A89NLS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 62.425, 140.967, 73.167 |
Unit cell angles | 90.00, 89.98, 90.00 |
Refinement procedure
Resolution | 19.818 - 2.300 |
R-factor | 0.1896 |
Rwork | 0.189 |
R-free | 0.20380 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ee4 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.145 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.820 | 19.820 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.150 | 0.480 |
Number of reflections | 55804 | |
<I/σ(I)> | 4.5 | 2 |
Completeness [%] | 99.5 | 98.7 |
Redundancy | 3.3 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 0.1 M BIS-TRIS PROPANE PH 7.0, 15% PEG 3350, 0.2 M NDSB-221 AND 0.2 M NAF |