4B7T
Glycogen Synthase Kinase 3 Beta complexed with Axin Peptide and Leucettine L4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 81.577, 81.577, 283.654 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.986 - 2.772 |
R-factor | 0.1973 |
Rwork | 0.195 |
R-free | 0.23530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1o9u |
RMSD bond length | 0.002 |
RMSD bond angle | 0.585 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.990 | 2.940 |
High resolution limit [Å] | 2.770 | 2.770 |
Rmerge | 0.060 | 0.270 |
Number of reflections | 14709 | |
<I/σ(I)> | 23.1 | 7.1 |
Completeness [%] | 97.3 | 91.1 |
Redundancy | 7.2 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.1 M TRIS-HCL, PH 8.0, 0.15 M MGCL2, 15% (W/V) PEG 4000 |