4B5F

Substrate bound Neisseria AP endonuclease in absence of metal ions (crystal form 1)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SRS BEAMLINE PX10.1
Synchrotron site	SRS
Beamline	PX10.1
Temperature [K]	100
Detector technology	CCD
Detector	MARMOSAIC 225 mm CCD
Spacegroup name	P 43 21 2
Unit cell lengths	67.789, 67.789, 125.165
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.895 - 2.005
R-factor	0.1825
Rwork	0.178
R-free	0.22680
Structure solution method	OTHER
Starting model (for MR)	NONE
RMSD bond length	0.004
RMSD bond angle	0.600
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	33.800
High resolution limit [Å]	2.000
Rmerge	0.110
Number of reflections	20280
Completeness [%]	100.0
Redundancy	6.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1