4B46
CetZ1 from Haloferax volcanii - GDP bound monomer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-02 |
Detector | ADSC QUANTUM CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.339, 62.214, 96.496 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.654 - 1.900 |
R-factor | 0.1753 |
Rwork | 0.174 |
R-free | 0.20710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PARTIAL MODEL OF CETZ4 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.036 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.650 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.110 | 0.580 |
Number of reflections | 27386 | |
<I/σ(I)> | 10 | 1.9 |
Completeness [%] | 99.8 | 99.4 |
Redundancy | 4.2 | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4 | 20% W/V PEG 6K, 1 M LITHIUM CHLORIDE, 0.1 M NA CITRATE PH 4 |