4B3C
Humanised monomeric RadA in complex with 5-hydroxy indole
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-09-19 |
Detector | RIGAKU RAXIS |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 70.560, 74.540, 41.170 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.560 - 1.900 |
R-factor | 0.2103 |
Rwork | 0.208 |
R-free | 0.26120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1PZN CHAIN A |
RMSD bond length | 0.010 |
RMSD bond angle | 1.186 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.130 | 2.000 |
High resolution limit [Å] | 1.890 | 1.890 |
Rmerge | 0.120 | 0.740 |
Number of reflections | 17821 | |
<I/σ(I)> | 14.65 | 2.55 |
Completeness [%] | 98.8 | 93 |
Redundancy | 6.6 | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.2 | 8% PEG1000, 100MM NA/K PHOSPHATE PH 6.2 |