4B23
Unprecedented sculpting of DNA at abasic sites by DNA glycosylase homolog Mag2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 120 |
Detector technology | CCD |
Detector | RAXIS IV |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 68.480, 84.520, 125.750 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.000 |
R-factor | 0.2481 |
Rwork | 0.248 |
R-free | 0.28980 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.006 |
RMSD bond angle | 1.185 |
Data reduction software | CrystalClear |
Data scaling software | CrystalClear |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 22272 | |
<I/σ(I)> | 8.4 | 2.7 |
Completeness [%] | 94.4 | 93.9 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 0.40 M (NH4) H2PO4 (NOT PH ADJUSTED), 6% 1,6-HEXANEDIOL |