4AZW
Crystal structure of monomeric WbdD.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 40.670, 89.600, 135.460 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 67.730 - 2.470 |
R-factor | 0.1928 |
Rwork | 0.190 |
R-free | 0.23744 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.014 |
RMSD bond angle | 1.673 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 67.700 |
High resolution limit [Å] | 2.470 |
Rmerge | 0.080 |
Number of reflections | 18171 |
<I/σ(I)> | 19.3 |
Completeness [%] | 98.5 |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |