4AZL
In meso structure of alginate transporter, AlgE, from Pseudomoas aeruginosa, PAO1, crystal form 2.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2010-03-05 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.090, 245.760, 47.130 |
Unit cell angles | 90.00, 104.36, 90.00 |
Refinement procedure
Resolution | 44.889 - 2.800 |
R-factor | 0.2393 |
Rwork | 0.237 |
R-free | 0.28030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rbh |
RMSD bond length | 0.006 |
RMSD bond angle | 1.218 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.900 | 2.950 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.220 | 0.910 |
Number of reflections | 23738 | |
<I/σ(I)> | 5.8 | 2 |
Completeness [%] | 93.2 | 95.3 |
Redundancy | 2.7 | 2.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.5 | 0.1 M SODIUM CACODYLATE, PH 6.5, 1.2 M SODIUM ACETATE |