4AXU
CRYSTAL STRUCTURE OF THAUMATIN FROM AN AUTO-HARVESTED CRYSTAL, control experiment
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID23-1 |
| Synchrotron site | ESRF |
| Beamline | ID23-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 58.007, 58.007, 150.522 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 45.940 - 1.380 |
| R-factor | 0.15015 |
| Rwork | 0.148 |
| R-free | 0.18920 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.023 |
| RMSD bond angle | 1.945 |
| Refinement software | REFMAC (5.6.0116) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 46.940 |
| High resolution limit [Å] | 1.380 |
| Rmerge | 0.010 |
| Number of reflections | 46432 |
| Completeness [%] | 86.0 |
| Redundancy | 10.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
