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4AXQ

CRYSTAL STRUCTURE OF ARCHAEMETZINCIN (AMZA) FROM ARCHAEOGLOBUS FULGIDUS AT 1.4 A RESOLUTION

Replaces:  2XHQ
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06DA
Synchrotron siteSLS
BeamlineX06DA
Temperature [K]293
Detector technologyCCD
DetectorMARMOSAIC 225 mm CCD
Spacegroup nameI 4
Unit cell lengths88.339, 88.339, 50.275
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution25.409 - 1.400
R-factor0.1652
Rwork0.164
R-free0.18640
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2x7m
RMSD bond length0.008
RMSD bond angle1.230
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]25.4001.480
High resolution limit [Å]1.4001.400
Rmerge0.0600.800
Number of reflections38202
<I/σ(I)>15.771.99
Completeness [%]99.598.6
Redundancy2.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
17.525% PEG 3350, 0.2 M (NH4)2SO4, 0.1 M HEPES PH 7.5

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PDB entries from 2024-10-30

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