4AX2
New Type VI-secreted toxins and self-resistance proteins in Serratia marcescens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 93 |
Detector technology | IMAGE PLATE |
Collection date | 2011-03-24 |
Detector | RIGAKU IMAGE PLATE |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 77.970, 77.970, 50.550 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 67.520 - 1.880 |
R-factor | 0.18187 |
Rwork | 0.180 |
R-free | 0.21898 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.010 |
RMSD bond angle | 1.249 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.500 | 1.980 |
High resolution limit [Å] | 1.880 | 1.880 |
Rmerge | 0.050 | 0.380 |
Number of reflections | 14813 | |
<I/σ(I)> | 26.6 | 5.9 |
Completeness [%] | 100.0 | 100 |
Redundancy | 11 | 10.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.55M LI2SO4, 5% PEG 8000, pH 7.5 |