4AWX
Moonlighting functions of FeoC in the regulation of ferrous iron transport in Feo
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13C1 |
Synchrotron site | NSRRC |
Beamline | BL13C1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 43 |
Unit cell lengths | 59.690, 59.690, 141.140 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.520 - 2.300 |
R-factor | 0.213 |
Rwork | 0.213 |
R-free | 0.22100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wia |
RMSD bond length | 0.009 |
RMSD bond angle | 1.700 |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.070 | 0.400 |
Number of reflections | 21747 | |
<I/σ(I)> | 28.02 | 3.05 |
Completeness [%] | 98.9 | 92.1 |
Redundancy | 4.7 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |