4AUW
CRYSTAL STRUCTURE OF THE BZIP HOMODIMERIC MAFB IN COMPLEX WITH THE C- MARE BINDING SITE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 94.964, 94.964, 200.111 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 85.750 - 2.900 |
R-factor | 0.25684 |
Rwork | 0.255 |
R-free | 0.29047 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 1.147 |
Refinement software | REFMAC (5.5.0102) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.000 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.080 | |
Number of reflections | 20968 | |
<I/σ(I)> | 7 | 1.8 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |