4AUQ
Structure of BIRC7-UbcH5b-Ub complex.
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Spacegroup name | P 43 21 2 |
格子定数 [Å] | 100.640, 100.640, 123.899 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 29.499 - 2.176 |
R因子 | 0.2044 |
Rwork | 0.202 |
R-free | 0.24950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 3A33 AND 3EB6 |
結合長の平均二乗偏差(RMSD) [Å] | 0.009 |
結合角の平均二乗偏差(RMSD) [度] | 1.239 |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 2.290 |
分解能 [Å] (高) | 2.180 | 2.180 |
Rmerge_l_obs | 0.060 | 0.620 |
独立反射数 | 33958 | |
<I/σ(I)> | 16.5 | 3.3 |
完全性 [%] | 99.8 | 99.2 |
冗長性 | 6.7 | 6.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 |