4ARV
Yersinia kristensenii phytase apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 345 mm plate |
Spacegroup name | P 1 |
Unit cell lengths | 55.410, 67.723, 73.164 |
Unit cell angles | 76.67, 87.35, 78.32 |
Refinement procedure
Resolution | 27.920 - 1.670 |
R-factor | 0.16538 |
Rwork | 0.164 |
R-free | 0.19847 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ars |
RMSD bond length | 0.017 |
RMSD bond angle | 1.805 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 1.750 | 1.750 |
High resolution limit [Å] | 1.660 | 1.660 |
Rmerge | 0.050 | 0.180 |
Number of reflections | 118484 | |
<I/σ(I)> | 24.9 | 4.9 |
Completeness [%] | 90.8 | 79.1 |
Redundancy | 5.6 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | PROTEIN CONCENTRATION 10MG/ML; CONDITION A12 FROM PACT SCREEN: SUCCINATE PHOSPHATE BORATE PH 5.0, 25% PEG1500 |