4AOM
MTIP and MyoA complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | RIGAKU SATURN 944 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.264, 54.704, 75.024 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 13.218 - 1.939 |
R-factor | 0.1788 |
Rwork | 0.177 |
R-free | 0.22310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qac |
RMSD bond length | 0.007 |
RMSD bond angle | 0.968 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 13.910 | 2.040 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.210 | 0.150 |
Number of reflections | 11754 | |
<I/σ(I)> | 10.8 | 5.4 |
Completeness [%] | 98.7 | 94.5 |
Redundancy | 4.1 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | 0.2M POTASSIUM THIOCYANATE, 20% PEG3350, pH 7.5 |