4AKI
Dynein Motor Domain - LuAc derivative
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2011-08-06 |
| Detector | ADSC CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 175.769, 118.186, 202.679 |
| Unit cell angles | 90.00, 90.91, 90.00 |
Refinement procedure
| Resolution | 49.140 - 3.700 |
| R-factor | 0.2335 |
| Rwork | 0.231 |
| R-free | 0.28903 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.511 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Refinement software | REFMAC (5.7.0019) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.130 | 3.770 |
| High resolution limit [Å] | 3.700 | 3.700 |
| Rmerge | 0.150 | |
| Number of reflections | 88918 | |
| <I/σ(I)> | 9.4 | 2 |
| Completeness [%] | 99.9 | 99.7 |
| Redundancy | 9.9 | 8.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
