4ACO
Structure of the budding yeast Ndc10 N-terminal domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.740, 87.760, 104.570 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 67.220 - 1.890 |
R-factor | 0.19443 |
Rwork | 0.193 |
R-free | 0.23159 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.020 |
RMSD bond angle | 2.034 |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 67.220 |
High resolution limit [Å] | 1.890 |
Rmerge | 0.050 |
Number of reflections | 39129 |
<I/σ(I)> | 13.4 |
Completeness [%] | 98.4 |
Redundancy | 3.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |