4ACB
CRYSTAL STRUCTURE OF TRANSLATION ELONGATION FACTOR SELB FROM METHANOCOCCUS MARIPALUDIS IN COMPLEX WITH THE GTP ANALOGUE GPPNHP
Replaces: 1WB3Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-12-19 |
Detector | MARRESEARCH |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 146.630, 146.630, 297.220 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.938 - 3.340 |
R-factor | 0.1809 |
Rwork | 0.179 |
R-free | 0.22330 |
Structure solution method | SAD |
Starting model (for MR) | 4ac9 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.150 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8_1069)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 3.540 |
High resolution limit [Å] | 3.340 | 3.340 |
Rmerge | 0.120 | 1.440 |
Number of reflections | 102021 | |
<I/σ(I)> | 9.24 | 1.36 |
Completeness [%] | 98.4 | 97.5 |
Redundancy | 4.6 | 4.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 10 MM KCL,20 MM TRIS/HCL (PH 7.5), 40 MM MGSO4, 2 MM DTT, 3 MM GDP, 1.8 - 2.0 M AMMONIUM SULFATE, 100 MM SODIUM CITRATE (PH 6.0), 1 MM DEOXYCHOLIC ACID |