4AC6
Corynebacterium glutamicum AcnR AU derivative structure
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-1 |
| Synchrotron site | ESRF |
| Beamline | ID14-1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-04-17 |
| Detector | ADSC CCD |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 34.142, 72.886, 73.250 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 73.250 - 2.540 |
| R-factor | 0.19792 |
| Rwork | 0.195 |
| R-free | 0.26336 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.355 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | SHELXCDE |
| Refinement software | REFMAC (5.6.0116) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 73.250 | 2.580 |
| High resolution limit [Å] | 2.540 | 2.540 |
| Rmerge | 0.070 | 0.150 |
| Number of reflections | 6461 | |
| <I/σ(I)> | 47.9 | 21.9 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 8.8 | 8.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4 | 1 M AMMONIUM PHOSPHATE, 100 MM SODIUM CITRATE PH 5.6 |
