4ABM
Crystal Structure of CHMP4B hairpin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 37.590, 71.430, 123.680 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 61.860 - 1.800 |
R-factor | 0.23043 |
Rwork | 0.228 |
R-free | 0.28517 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.018 |
RMSD bond angle | 0.884 |
Data scaling software | iMOSFLM |
Phasing software | SHELX |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.230 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.270 | 0.410 |
Number of reflections | 30007 | |
<I/σ(I)> | 16.3 | 4.4 |
Completeness [%] | 99.6 | 100 |
Redundancy | 7.8 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |