4AB5
Regulatory domain structure of NMB2055 (MetR) a LysR family regulator from N. meningitidis
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BM14 |
| Synchrotron site | ESRF |
| Beamline | BM14 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | MARMOSAIC 225 mm CCD |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 65.140, 52.570, 65.890 |
| Unit cell angles | 90.00, 94.09, 90.00 |
Refinement procedure
| Resolution | 21.580 - 2.510 |
| R-factor | 0.1887 |
| Rwork | 0.186 |
| R-free | 0.23770 |
| Structure solution method | MAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.120 |
| Refinement software | BUSTER (2.11.2) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.500 |
| Rmerge | 0.100 |
| Number of reflections | 13879 |
| Completeness [%] | 90.0 |
| Redundancy | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
