4A9Z

CRYSTAL STRUCTURE OF HUMAN P63 TETRAMERIZATION DOMAIN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I02
Synchrotron site	Diamond
Beamline	I02
Temperature [K]	100
Detector technology	CCD
Collection date	2011-10-21
Detector	ADSC CCD
Spacegroup name	P 31 2 1
Unit cell lengths	80.850, 80.850, 68.370
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	48.920 - 2.290
R-factor	0.1967
Rwork	0.194
R-free	0.24590
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.010
RMSD bond angle	0.980
Data reduction software	MOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	BUSTER (2.10.0)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	70.020	2.410
High resolution limit [Å]	2.290	2.290
Rmerge	0.050	0.980
Number of reflections	11980
<I/σ(I)>	15.7	2.1
Completeness [%]	100.0	100
Redundancy	10.2	8.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1