4A9V
Pseudomonas fluorescens PhoX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-11-11 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.820, 75.980, 114.970 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.300 - 1.100 |
R-factor | 0.11836 |
Rwork | 0.137 |
R-free | 0.11740 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3zwu |
RMSD bond length | 0.006 |
RMSD bond angle | 1.082 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.300 | 1.120 |
High resolution limit [Å] | 1.100 | 1.100 |
Rmerge | 0.120 | 0.440 |
Number of reflections | 252884 | |
<I/σ(I)> | 8.1 | 2.3 |
Completeness [%] | 99.7 | 97.4 |
Redundancy | 6.1 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.9 | 19% PEG 6000, 0.1 M TRIS PH 7.9, 0.2 M LICL, 300 UM CACL2 |