4A6Y
CRYSTAL STRUCTURE OF FAB FRAGMENT OF ANTI-(4-HYDROXY-3-NITROPHENYL) -ACETYL MURINE GERMLINE ANTIBODY BBE6.12H3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 2006-06-15 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 86.283, 81.418, 128.911 |
Unit cell angles | 90.00, 90.50, 90.00 |
Refinement procedure
Resolution | 23.020 - 2.900 |
R-factor | 0.24 |
Rwork | 0.240 |
R-free | 0.26000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ngq |
RMSD bond length | 0.009 |
RMSD bond angle | 1.700 |
Data reduction software | AUTOMAR |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | CNS (1.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.080 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.120 | 0.420 |
Number of reflections | 19688 | |
<I/σ(I)> | 4.7 | 2.6 |
Completeness [%] | 93.5 | 87.3 |
Redundancy | 3 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.1 | 21% PEG 3350 IN 0.05 M TRIS, PH 7.1 |