4A6H
Crystal structure of Slm1-PH domain in complex with Inositol-4- phosphate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-15 |
Detector | ADSC QUANTUM 315r |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.000, 71.600, 82.700 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.808 - 1.449 |
R-factor | 0.1935 |
Rwork | 0.193 |
R-free | 0.22620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | APO STRUCTURE |
RMSD bond length | 0.006 |
RMSD bond angle | 1.014 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: 1.5_2)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.050 | 0.350 |
Number of reflections | 80522 | |
<I/σ(I)> | 18.8 | 4.01 |
Completeness [%] | 99.2 | 96 |
Redundancy | 3.7 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |