4A6F
Crystal structure of Slm1-PH domain in complex with Phosphoserine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-10-09 |
Detector | MARRESEARCH |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 37.540, 73.650, 82.470 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.933 - 1.680 |
R-factor | 0.2155 |
Rwork | 0.214 |
R-free | 0.24160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4a5k |
RMSD bond length | 0.006 |
RMSD bond angle | 1.107 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: 1.5_2)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.800 |
High resolution limit [Å] | 1.680 | 1.680 |
Rmerge | 0.100 | 0.500 |
Number of reflections | 26485 | |
<I/σ(I)> | 10.61 | 2.34 |
Completeness [%] | 98.7 | 93.4 |
Redundancy | 5.4 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.5 | pH 7.5 |