4A4X
NEK2-EDE bound to CCT248662
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 101.223, 56.909, 74.408 |
Unit cell angles | 90.00, 127.12, 90.00 |
Refinement procedure
Resolution | 50.379 - 2.400 |
R-factor | 0.2065 |
Rwork | 0.204 |
R-free | 0.24690 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.016 |
RMSD bond angle | 1.597 |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.380 |
High resolution limit [Å] | 2.400 |
Rmerge | 0.110 |
Number of reflections | 13251 |
<I/σ(I)> | 7.5 |
Completeness [%] | 99.4 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |