4A48
Crosstalk between Cu(I) and Zn(II) homeostasis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-30 |
Detector | ADSC CCD |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 24.660, 52.600, 39.920 |
Unit cell angles | 90.00, 98.13, 90.00 |
Refinement procedure
Resolution | 39.520 - 1.400 |
R-factor | 0.14263 |
Rwork | 0.140 |
R-free | 0.19527 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xmw |
RMSD bond length | 0.011 |
RMSD bond angle | 1.525 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 31.590 | 1.480 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.050 | 0.220 |
Number of reflections | 18146 | |
<I/σ(I)> | 15.3 | 5.1 |
Completeness [%] | 91.4 | 86.2 |
Redundancy | 4 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 200 MM NAF, 20% (W/V) PEG 3350 |