4A47
Crosstalk between Cu(I) and Zn(II) homeostasis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-05-30 |
Detector | ADSC CCD |
Spacegroup name | H 3 2 |
Unit cell lengths | 85.620, 85.620, 188.142 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 68.980 - 1.900 |
R-factor | 0.19706 |
Rwork | 0.195 |
R-free | 0.24302 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xmt |
RMSD bond length | 0.012 |
RMSD bond angle | 1.471 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.810 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.090 | 0.370 |
Number of reflections | 21226 | |
<I/σ(I)> | 10.9 | 4.1 |
Completeness [%] | 99.8 | 100 |
Redundancy | 5.7 | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 1.6 M TRISODIUM CITRATE, PH 6.5. |