4A2N
Crystal Structure of Ma-ICMT
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-10-04 |
| Detector | ADSC CCD |
| Spacegroup name | P 62 2 2 |
| Unit cell lengths | 114.920, 114.920, 169.291 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 38.947 - 3.400 |
| R-factor | 0.24 |
| Rwork | 0.238 |
| R-free | 0.27490 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.341 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHENIX |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.540 | 3.580 |
| High resolution limit [Å] | 3.400 | 3.400 |
| Rmerge | 0.130 | 0.860 |
| Number of reflections | 9625 | |
| <I/σ(I)> | 9.3 | 2.1 |
| Completeness [%] | 98.3 | 99 |
| Redundancy | 6.7 | 7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 0.1 M AMMONIUM SULPHATE, 0.3 M SODIUM FORMATE, 0.1 M SODIUM CACODYLATE PH 6.5, 3% (V/V) POLYGLUTAMIC ACID AND 20%-26% (W/V) PEG 550 MME |
