4A2G
Coriolopsis gallica laccase collected at 8.98 keV
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X6A |
Synchrotron site | NSLS |
Beamline | X6A |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.011, 85.230, 151.514 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 75.760 - 1.800 |
R-factor | 0.15856 |
Rwork | 0.157 |
R-free | 0.18793 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.027 |
RMSD bond angle | 2.062 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0110) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.700 | 1.900 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.040 | 0.180 |
Number of reflections | 64137 | |
<I/σ(I)> | 11.2 | 4.2 |
Completeness [%] | 95.2 | 95 |
Redundancy | 2.5 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 10% PEG 1000, 10% PEG 8000, TRIS PH 7.2 . |